1H and 13C NMR assignments of the antitumor macrolide bryostatin 1

Daniel E. Schaufelberger, Gwendolyn N. Chmurny, Mary P. Koleck

Research output: Contribution to journalArticlepeer-review

Abstract

During a large‐scale isolation of bryostatin 1, NMR measurements indicated that parts of the published 13C and 1H NMR assignments had to be revised. These reassignments were based on extensive homonuclear and heteronuclear one‐ and two‐dimensional NMR techniques performed at 500 MHz. These independently obtained assignments are also in good agreement with the revised assignments and structure of bryostatin 3.

Original languageEnglish (US)
Pages (from-to)366-374
Number of pages9
JournalMagnetic Resonance in Chemistry
Volume29
Issue number4
DOIs
StatePublished - Apr 1991
Externally publishedYes

Keywords

  • Bryostatin 1
  • NMR data
  • Structure

ASJC Scopus subject areas

  • Chemistry(all)
  • Materials Science(all)

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