Principles and applications of a research-oriented gas chromatography-mass spectrometry data system

J. E. Campana, Terence H Risby, P. C. Jurs

Research output: Contribution to journalArticle

Abstract

A research-oriented gas chromatography-mass spectrometry data system for a quadrupole mass spectrometer has been developed based on a centrally located departmental computer facility. An overview of the hardware and software system is presented, emphasizing the important aspects of on-line computer data acquisition and control and the design philosophy used in the development of the system. The application of the system is demonstrated by the g.c.-m.s. analysis of a mixture of four transition metal β-diketonates (Al, Cr, Rh, and Ru tris-1,1,1-trifluoro-pentane-2,4-dionate). This analysis involved vacuum gas chromatography with a support-coated open tubular column and detection of the eluent by chemical ionization mass spectrometry. The results demonstrate the data system capabilities and indicate the utility of the combined methodologies.

Original languageEnglish (US)
Pages (from-to)321-340
Number of pages20
JournalAnalytica Chimica Acta
Volume112
Issue number4
DOIs
StatePublished - Dec 15 1979
Externally publishedYes

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Information Systems
Gas chromatography
Gas Chromatography-Mass Spectrometry
Mass spectrometry
gas chromatography
mass spectrometry
transition element
Mass spectrometers
Vacuum
Research
Gas Chromatography
data acquisition
Computer hardware
hardware
Ionization
Transition metals
Data acquisition
Mass Spectrometry
ionization
Computer systems

ASJC Scopus subject areas

  • Biochemistry
  • Analytical Chemistry
  • Spectroscopy
  • Environmental Chemistry

Cite this

Principles and applications of a research-oriented gas chromatography-mass spectrometry data system. / Campana, J. E.; Risby, Terence H; Jurs, P. C.

In: Analytica Chimica Acta, Vol. 112, No. 4, 15.12.1979, p. 321-340.

Research output: Contribution to journalArticle

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