A Solid sampled reactor-injection vessel for gas chromatography

R. M. Dagnall; B. Fleet; T. H. Risby

doi:10.1080/00032717008067791

A Solid sampled reactor-injection vessel for gas chromatography

R. M. Dagnall, B. Fleet, T. H. Risby

Research output: Contribution to journal › Article › peer-review

Abstract

The design and construction of a reactor injection assembly for the formation of volatile metal fluorides is described. The sample, in a chlorine trifluoride atmosphere, is heated with a radio-frequency induction heater and the volatile products passed into a hydrogen diffusion flame emission detector. Although this device is primarily intended for use in gas chromatography, this preliminary evaluation is concerned with its application to atomic spectroscopy.

Original language	English (US)
Pages (from-to)	143-150
Number of pages	8
Journal	Analytical Letters
Volume	3
Issue number	3
DOIs	https://doi.org/10.1080/00032717008067791
State	Published - Jan 1 1970
Externally published	Yes

Keywords

boron
gas-chromatography
metal fluorides
molecular emission
solid sample reactor

ASJC Scopus subject areas

Analytical Chemistry
Biochemistry
Spectroscopy
Clinical Biochemistry
Biochemistry, medical
Electrochemistry

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AB - The design and construction of a reactor injection assembly for the formation of volatile metal fluorides is described. The sample, in a chlorine trifluoride atmosphere, is heated with a radio-frequency induction heater and the volatile products passed into a hydrogen diffusion flame emission detector. Although this device is primarily intended for use in gas chromatography, this preliminary evaluation is concerned with its application to atomic spectroscopy.

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KW - gas-chromatography

KW - metal fluorides

KW - molecular emission

KW - solid sample reactor

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A Solid sampled reactor-injection vessel for gas chromatography

Abstract

Keywords

ASJC Scopus subject areas

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